diff --git a/python/sglang/srt/layers/attention/nsa/quant_k_cache.py b/python/sglang/srt/layers/attention/nsa/quant_k_cache.py
index 320936cf5..a7dc745c2 100644
--- a/python/sglang/srt/layers/attention/nsa/quant_k_cache.py
+++ b/python/sglang/srt/layers/attention/nsa/quant_k_cache.py
@@ -13,6 +13,84 @@ def quantize_k_cache(cache_k):
         return _quantize_k_cache_slow(cache_k)
 
 
+def quantize_k_cache_separate(
+    k_nope: torch.Tensor,
+    k_rope: torch.Tensor,
+    tile_size: int = 128,
+):
+    """
+    Quantize k_nope and k_rope separately without concat, returns two tensors.
+
+    This avoids the concat operation and enables direct reuse of set_mla_kv_buffer_triton
+    by returning two separate byte tensors for the nope and rope parts.
+
+    Args:
+        k_nope: (num_tokens, dim_nope) or (num_tokens, 1, dim_nope)
+                Must have dim_nope=512 for FP8 MLA quantization
+        k_rope: (num_tokens, dim_rope) or (num_tokens, 1, dim_rope)
+                Must have dim_rope=64 for FP8 MLA quantization
+        tile_size: quantization tile size (default 128)
+
+    Returns:
+        Tuple of (nope_part, rope_part) where:
+        - nope_part: (num_tokens, 1, 528) as uint8 view, contains [nope_fp8(512) | scales(16)]
+        - rope_part: (num_tokens, 1, 128) as uint8 view, contains [rope_bf16_bytes(128)]
+
+        These two tensors can be directly passed to set_mla_kv_buffer_triton(kv_buffer, loc, nope_part, rope_part)
+    """
+    # Squeeze middle dimension if present
+    k_nope_2d = k_nope.squeeze(1) if k_nope.ndim == 3 else k_nope
+    k_rope_2d = k_rope.squeeze(1) if k_rope.ndim == 3 else k_rope
+
+    num_tokens = k_nope_2d.shape[0]
+    dim_nope = k_nope_2d.shape[1]
+    dim_rope = k_rope_2d.shape[1]
+
+    # Validate dimensions for FP8 MLA
+    if dim_nope != 512:
+        raise ValueError(f"Expected dim_nope=512 for FP8 MLA, got {dim_nope}")
+    if dim_rope != 64:
+        raise ValueError(f"Expected dim_rope=64 for FP8 MLA, got {dim_rope}")
+    if k_rope_2d.shape[0] != num_tokens:
+        raise ValueError(
+            f"k_nope and k_rope must have same num_tokens, got {num_tokens} vs {k_rope_2d.shape[0]}"
+        )
+
+    # Call fast kernel that directly produces two separate outputs (single Triton kernel)
+    if NSA_QUANT_K_CACHE_FAST:
+        nope_part, rope_part = _quantize_k_cache_fast_separate(
+            k_nope=k_nope_2d, k_rope=k_rope_2d, group_size=tile_size
+        )
+    else:
+        # Fallback: use existing slow path with post-processing
+        cache_k_concat = torch.cat([k_nope_2d, k_rope_2d], dim=-1)
+        packed_output_4d = quantize_k_cache(cache_k_concat.unsqueeze(1).unsqueeze(1))
+        packed_output = packed_output_4d.squeeze(1).squeeze(1)
+
+        # Convert to uint8 bytes view
+        packed_bytes = packed_output.contiguous().view(torch.uint8)
+
+        # Strict byte-size validation
+        expected_total_bytes = 656  # 512 (nope_fp8) + 16 (scales) + 128 (rope_bf16)
+        if packed_bytes.shape[1] != expected_total_bytes:
+            raise ValueError(
+                f"Packed output has {packed_bytes.shape[1]} bytes, expected {expected_total_bytes}. "
+                f"Original dtype: {packed_output.dtype}, shape: {packed_output.shape}"
+            )
+
+        # Split into nope and rope parts
+        num_tiles = dim_nope // tile_size  # 4
+        nope_part_bytes = dim_nope + num_tiles * 4  # 512 + 16 = 528
+        rope_part_bytes = 128
+
+        nope_part = packed_bytes[:, :nope_part_bytes].unsqueeze(1)
+        rope_part = packed_bytes[
+            :, nope_part_bytes : nope_part_bytes + rope_part_bytes
+        ].unsqueeze(1)
+
+    return nope_part, rope_part
+
+
 # Copied from original
 def _quantize_k_cache_slow(
     input_k_cache: torch.Tensor,  # (num_blocks, block_size, h_k, d)
@@ -145,6 +223,83 @@ def _quantize_k_cache_fast(k_nope, k_rope, group_size: int = 128):
     return output
 
 
+def _quantize_k_cache_fast_separate(k_nope, k_rope, group_size: int = 128):
+    """
+    Quantize k_nope and k_rope in a single Triton kernel, directly outputting two separate tensors.
+
+    This avoids packing/unpacking and enables direct use with set_mla_kv_buffer_triton.
+
+    :param k_nope: (num_tokens, dim_nope 512) bfloat16
+    :param k_rope: (num_tokens, dim_rope 64) bfloat16
+    :param group_size: quantization tile size (default 128, kernel is tuned for this value)
+    :return: Tuple of (nope_part_u8, rope_part_u8)
+        - nope_part_u8: (num_tokens, 1, nope_part_bytes) uint8, layout [nope_fp8(dim_nope) | scales(num_tiles*4)]
+        - rope_part_u8: (num_tokens, 1, rope_part_bytes) uint8, layout [rope_bf16_bytes(dim_rope*2)]
+    """
+    num_tokens, dim_nope = k_nope.shape
+    num_tokens_, dim_rope = k_rope.shape
+
+    assert num_tokens == num_tokens_, f"k_nope and k_rope must have same num_tokens"
+
+    # Ensure contiguous tensors for kernel
+    k_nope = k_nope.contiguous()
+    k_rope = k_rope.contiguous()
+
+    num_tiles = dim_nope // group_size
+
+    # Calculate byte sizes based on validated dimensions
+    # nope_part: [FP8 quantized data (dim_nope bytes)] + [FP32 scales (num_tiles * 4 bytes)]
+    # rope_part: [BF16 raw data (dim_rope * 2 bytes)]
+    nope_part_bytes = (
+        dim_nope + num_tiles * 4
+    )  # e.g., 512 + 4*4 = 528 for dim_nope=512, group_size=128
+    rope_part_bytes = (
+        dim_rope * k_rope.element_size()
+    )  # e.g., 64 * 2 = 128 for dim_rope=64, BF16
+
+    # Allocate two separate output buffers (as uint8 for direct byte-level access)
+    nope_part_u8 = torch.empty(
+        (num_tokens, nope_part_bytes), dtype=torch.uint8, device=k_nope.device
+    )
+    rope_part_u8 = torch.empty(
+        (num_tokens, rope_part_bytes), dtype=torch.uint8, device=k_rope.device
+    )
+
+    # Create typed views for the kernel to write into
+    # Fixed byte layout for nope_part: [nope_fp8 (dim_nope bytes) | scales_fp32 (num_tiles*4 bytes)]
+    # Fixed byte layout for rope_part: [rope_bf16 (dim_rope*2 bytes)]
+    nope_q_view = nope_part_u8[:, :dim_nope].view(torch.float8_e4m3fn)
+    nope_s_view = nope_part_u8[:, dim_nope:].view(torch.float32)
+    rope_view = rope_part_u8.view(torch.bfloat16)
+
+    # Kernel launch parameters
+    num_blocks_per_token = triton.cdiv(dim_nope + dim_rope, group_size)
+    NUM_NOPE_BLOCKS = dim_nope // group_size
+
+    # Use the same kernel as _quantize_k_cache_fast (reuse existing implementation)
+    _quantize_k_cache_fast_kernel[(num_tokens, num_blocks_per_token)](
+        nope_q_view,
+        nope_s_view,
+        rope_view,
+        k_nope,
+        k_rope,
+        nope_q_view.stride(0),
+        nope_s_view.stride(0),
+        rope_view.stride(0),
+        k_nope.stride(0),
+        k_rope.stride(0),
+        NUM_NOPE_BLOCKS=NUM_NOPE_BLOCKS,
+        GROUP_SIZE=group_size,
+        DIM_NOPE=dim_nope,
+        DIM_ROPE=dim_rope,
+        FP8_MIN=torch.finfo(torch.float8_e4m3fn).min,
+        FP8_MAX=torch.finfo(torch.float8_e4m3fn).max,
+    )
+
+    # Add middle dimension for compatibility with set_mla_kv_buffer_triton
+    return nope_part_u8.unsqueeze(1), rope_part_u8.unsqueeze(1)
+
+
 @triton.jit
 def _quantize_k_cache_fast_kernel(
     output_nope_q_ptr,
@@ -255,7 +410,50 @@ if __name__ == "__main__":
         )
 
     print("Passed")
-    print("Do benchmark...")
+
+    # Test quantize_k_cache_separate: verify output matches concat path
+    print("\nTesting quantize_k_cache_separate...")
+    for num_tokens in [64, 100]:
+        dim_nope = 512
+        dim_rope = 64
+
+        k_nope = torch.randn(
+            num_tokens, 1, dim_nope, dtype=torch.bfloat16, device="cuda"
+        )
+        k_rope = torch.randn(
+            num_tokens, 1, dim_rope, dtype=torch.bfloat16, device="cuda"
+        )
+
+        # Old path: concat then quantize
+        k_concat = torch.cat([k_nope, k_rope], dim=-1).squeeze(1)  # (num_tokens, 576)
+        old_output = quantize_k_cache(k_concat.unsqueeze(1).unsqueeze(1))  # 4D input
+        old_output = old_output.squeeze(1).squeeze(1)  # Back to (num_tokens, 656)
+
+        # New path: quantize separately
+        nope_part, rope_part = quantize_k_cache_separate(k_nope, k_rope)
+        new_bytes = torch.cat([nope_part.squeeze(1), rope_part.squeeze(1)], dim=-1)
+
+        # Compare byte-level equality
+        old_bytes = old_output.view(torch.uint8)
+
+        if old_bytes.shape != new_bytes.shape:
+            raise RuntimeError(
+                f"Shape mismatch: {old_bytes.shape} vs {new_bytes.shape}"
+            )
+
+        diff_bytes = (old_bytes != new_bytes).sum().item()
+        if diff_bytes > 0:
+            max_diff = (old_bytes.float() - new_bytes.float()).abs().max().item()
+            raise RuntimeError(
+                f"quantize_k_cache_separate output doesn't match concat path: "
+                f"{diff_bytes} differing bytes, max_diff={max_diff}"
+            )
+
+        print(f"  num_tokens={num_tokens}: PASSED (outputs match byte-wise)")
+
+    print("quantize_k_cache_separate tests passed!")
+
+    print("\nDo benchmark...")
 
     for num_blocks, block_size in [
         (1, 64),
diff --git a/python/sglang/srt/mem_cache/memory_pool.py b/python/sglang/srt/mem_cache/memory_pool.py
index f095d1c1f..11446e102 100644
--- a/python/sglang/srt/mem_cache/memory_pool.py
+++ b/python/sglang/srt/mem_cache/memory_pool.py
@@ -22,7 +22,10 @@ from typing import List
 from sglang.srt.configs.mamba_utils import BaseLinearStateParams
 from sglang.srt.environ import envs
 from sglang.srt.layers.attention.nsa import index_buf_accessor
-from sglang.srt.layers.attention.nsa.quant_k_cache import quantize_k_cache
+from sglang.srt.layers.attention.nsa.quant_k_cache import (
+    quantize_k_cache,
+    quantize_k_cache_separate,
+)
 from sglang.srt.utils.torch_memory_saver_adapter import TorchMemorySaverAdapter
 
 """
@@ -1597,12 +1600,22 @@ class MLATokenToKVPool(KVCache):
         layer_id = layer.layer_id
 
         if self.use_nsa and self.nsa_kv_cache_store_fp8:
-            # original cache_k: (num_tokens, num_heads 1, hidden 576); we unsqueeze the page_size=1 dim here
-            # TODO no need to cat
-            cache_k = torch.cat([cache_k_nope, cache_k_rope], dim=-1)
-            cache_k = quantize_k_cache(cache_k.unsqueeze(1)).squeeze(1)
-            cache_k = cache_k.view(self.store_dtype)
-            self.kv_buffer[layer_id - self.start_layer][loc] = cache_k
+            # OPTIMIZATION: Quantize k_nope and k_rope separately to avoid concat overhead
+            # This also enables reuse of set_mla_kv_buffer_triton two-tensor write path
+            # quantize_k_cache_separate returns (nope_part, rope_part) as uint8 bytes
+            cache_k_nope_fp8, cache_k_rope_fp8 = quantize_k_cache_separate(
+                cache_k_nope, cache_k_rope
+            )
+
+            # Reuse existing two-tensor write kernel (works with FP8 byte layout)
+            # cache_k_nope_fp8: (num_tokens, 1, 528) uint8 [nope_fp8(512) | scales(16)]
+            # cache_k_rope_fp8: (num_tokens, 1, 128) uint8 [rope_bf16_bytes(128)]
+            set_mla_kv_buffer_triton(
+                self.kv_buffer[layer_id - self.start_layer],
+                loc,
+                cache_k_nope_fp8,
+                cache_k_rope_fp8,
+            )
         else:
             if cache_k_nope.dtype != self.dtype:
                 cache_k_nope = cache_k_nope.to(self.dtype)
diff --git a/python/sglang/srt/mem_cache/utils.py b/python/sglang/srt/mem_cache/utils.py
index 361accb87..3aec3dd89 100644
--- a/python/sglang/srt/mem_cache/utils.py
+++ b/python/sglang/srt/mem_cache/utils.py
@@ -46,17 +46,38 @@ def set_mla_kv_buffer_kernel(
     loc = tl.load(loc_ptr + pid_loc).to(tl.int64)
     dst_ptr = kv_buffer_ptr + loc * buffer_stride + offs
 
+    # Three-way branch to handle boundary correctly while preserving fast path
     if base + BLOCK <= nope_dim:
+        # Fast path: entire block is in nope region
         src = tl.load(
             cache_k_nope_ptr + pid_loc * nope_stride + offs,
             mask=mask,
         )
-    else:
+    elif base >= nope_dim:
+        # Fast path: entire block is in rope region
         offs_rope = offs - nope_dim
         src = tl.load(
             cache_k_rope_ptr + pid_loc * rope_stride + offs_rope,
             mask=mask,
         )
+    else:
+        # Boundary case: block spans nope/rope boundary (e.g., FP8 with nope_dim=528)
+        # Handle each offset individually to avoid negative indexing
+        is_nope = offs < nope_dim
+        is_rope = (offs >= nope_dim) & (offs < (nope_dim + rope_dim))
+
+        src_nope = tl.load(
+            cache_k_nope_ptr + pid_loc * nope_stride + offs,
+            mask=mask & is_nope,
+            other=0,
+        )
+        src_rope = tl.load(
+            cache_k_rope_ptr + pid_loc * rope_stride + (offs - nope_dim),
+            mask=mask & is_rope,
+            other=0,
+        )
+
+        src = tl.where(is_nope, src_nope, src_rope)
 
     tl.store(dst_ptr, src, mask=mask)